مساهمة تحليلية لمقايسة بعض مركبات ن-نتروزأمين الطيارة في اللحوم باستخدام طريقة الكروماتوغرافيا الغازية ومتحري التأين اللهبي

Authors

  • زيد العساف
  • فرانسواه قره بيت
  • محمد القسيم

Abstract

تم تحديد شروط الفصل المثلى من أجل التحليل الكمي لمركبات ن-نتروزأمين الطيارة Volatile N-nitrosamines من عينات اللحوم  ومنتجاتها بطريقة الكروماتوغرافيا الغازية Gas Chromatography (GC) المجهزة بمتحرٍّ (مكشاف) التأين اللهبي Flame ionization Detector (FID) باستخدام عمود Optima XLB (30m × 0.25 mm × 0.25µm ). أظهرت النتائج أن الطريقة ذات حد كشف منخفض (LOD) وأنها ذات خطيةLinearity  وتكرارية repeatability مع معدل للاستردادية Recovery  تراوح بين 89% و 105.5% وقيم مقبولة للانحراف المعياري النسبي RSD.

Conditions for Gas chromatography (GC) equipped with Flame Ionization Detector (FID) were optimized in order to dtermine volatile N-nitrosamine in meat and meat products, using optima XLB (30m × 0.25 mm × 0.25µm) column. Results reveal that the method has a low detection limit with repeatability and linearity and with average recovery ranging from 89%  to 105.5% and accepted relative standard deviation.

Author Biographies

زيد العساف

كلية الصيدلة- جامعة دمشق – دمشق- سورية.

فرانسواه قره بيت

كلية العلوم - جامعة دمشق- دمشق - سورية.

محمد القسيم

- كلية الصيدلة- جامعة دمشق- دمشق،  سورية.

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Published

2014-01-21

How to Cite

1.
العساف ز, قره بيت ف, القسيم م. مساهمة تحليلية لمقايسة بعض مركبات ن-نتروزأمين الطيارة في اللحوم باستخدام طريقة الكروماتوغرافيا الغازية ومتحري التأين اللهبي. Tuj-hlth [Internet]. 2014Jan.21 [cited 2025Apr.18];36(1). Available from: https://journal.tishreen.edu.sy/index.php/hlthscnc/article/view/738

Issue

Vol. 36 No. 1 (2014): العلوم الصحية

Section

Articles

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