Choosing The Optimal Extraction Condition by Ultrasonic and Soxhlet for Determination of Dimethoate in Agricultural Soil Samples By HPLC

Authors

  • Mohammad Maarouf Tishreen University
  • Tareq Arraj Tishreen University
  • Ali Al Shaer Tishreen University

Abstract

In this research, the best method for extraction Dimethoate pesticide from agricultural soil samples taken from greenhouses in the Burj Islam area located in Lattakia Governorate was determined, in addition to determining the appropriate wavelength for analysis using a high-performance liquid chromatography.

The results of the analysis, using different mixtures of solvents (hexan:aceton – double distilled water:methanol- methanol:dichloromethane- double distilled water) showed that the best mixture was( hexane: acetone 1:1) by applied two extraction methods Ultrasonic-Soxhlet, the Ultrasonic waves were the best, as the analysis was performed with different wavelengths (240 - 225 - 205 - 200) nm, the best of which was (200 nm) . The recovery ranged between 99,47 and 106,38%, The limits of Detection (LOD) are 0,02 ppb , and the limit Quantitative Detection (LQD) are 0,068 ppb.

 

Author Biographies

Mohammad Maarouf, Tishreen University

Professor. Faculty of science- Department of Chemistry

Tareq Arraj, Tishreen University

Doctor. Higher Institute for Environment research,

Ali Al Shaer, Tishreen University

Postgraduate student-.faculty of science- Department of Chemistry

Downloads

Published

2021-03-30

How to Cite

1.
معروف م, عراج ط, الشاعر ع. Choosing The Optimal Extraction Condition by Ultrasonic and Soxhlet for Determination of Dimethoate in Agricultural Soil Samples By HPLC . TUJ-BA [Internet]. 2021Mar.30 [cited 2024Dec.28];43(1). Available from: https://journal.tishreen.edu.sy/index.php/bassnc/article/view/10466

Issue

Vol. 43 No. 1 (2021): Tishreen University Journal for Research and Scientific Studies - Basic Sciences Series

Section

Articles

License

Creative Commons License

This work is licensed under a Creative Commons Attribution-NonCommercial-ShareAlike 4.0 International License.

The authors retain the copyright and grant the right to publish in the magazine for the first time with the transfer of the commercial right to the Tishreen University Journal -Basic Sciences Series  

 Under a CC BY- NC-SA 04 license that allows others to share the work with of the work's authorship and initial publication in this journal. Authors can use a copy of their articles in their scientific activity, and on their scientific websites, provided that the place of publication is indicted in Tishreen University Journal -Basic Sciences Series .  The Readers have the right to send, print and subscribe to the initial version of the article, and the title of Tishreen University Journal -Basic Sciences Series   Publisher

 

journal uses a CC BY-NC-SA license which mean

You are free to:

  • Adapt — remix, transform, and build upon the material
  •  
  • The licensor cannot revoke these freedoms as long as you follow the license terms.

 

  • Attribution — You must give appropriate credit, provide a link to the license, and indicate if changes were made. You may do so in any reasonable manner, but not in any way that suggests the licensor endorses you or your use.
  • NonCommercial — You may not use the material for commercial purposes.
  • ShareAlike — If you remix, transform, or build upon the material, you must distribute your contributions under the same license as the original.
  • No additional restrictions — You may not apply legal terms or technological measures that legally restrict others from doing anything the license permits.

Most read articles by the same author(s)

1 2 3 > >>